low & high pressure automated reaction calorimeter
SIMULARReaction Calorimetry
...an essential tool for Process R&DA reaction calorimeter is a
tool that allows for the precise simulation and thermal study of a
chemistry and associated plant, typically at the one litre scale.
Subsequently, important safety, viability and optimisation data can
be obtained prior to scale up.Safe process scale-up
The most common application of a reaction calorimeter is the
determination of heat released during a process. From this the
subsequent cooling duty required for scale up can be calculated. In
addition the potential adiabatic temperature rise can be
calculated. Combined with other techniques, a basis for safety can
therefore be determined.Further information available includes the
determination of reagent accumulation and the impact of variables
such as agitation and catalyst upon the reaction rate. By changing
feed rates and batch temperature, the optimum operating conditions
for both efficiency and product quality, can be
determined.Flexibility without compromise
SIMULAR is built around our unique modular electronics and the
latest in-house developed Windows software, to provide you with a
tool that meets your requirements, both now, and into the
future.Select the components that most closely match your plant
conditions, then combine them to have a dedicated, simple-to
operate tool that simulates your plant and process.This includes
temperature range, agitation, speed, reagent feed rate and even
reactor geometry - find out why we offer the best, most flexible,
reaction calorimeter for your application.Multiple calorimetric
methods
Unlike most leading reaction calorimeters, SIMULAR is designed to
be used by research chemists and safety specialists alike.This is
made possible by power compensation calorimetry, unique to the
SIMULAR.This allows accurate determination of heat release without
the need for time-consuming calibration or complex calculation
procedures.For more conservative users, the classical heat flow
calorimetry method is also supported as standard.WHY
SIMULAR?Flexible:
Whether it is the wide temperature options,multiple reagent feeds
or reactor specifications, no other system covers such a wide range
of chemical conditions and variables.Powerful:
SIMULAR is the only reaction calorimeter to offer Heat Flow, Power
Compensation and Reflux Calorimetric techniques. Each of which
offers specific advantages depending on your chemistry, and all are
available regardless of reactor specification.Expandable:
The modularity of SIMULAR systems allows you to add on to your
system - feeds, sensors etc - in the future simply and without
major cost implications.Ease of ownership:
The system will fit into existing fume hoods and usually needs only
existing power supplies.We also have the most innovative and user
friendly software, and use the standard laboratory components that
you are already familiar with.DON¡¯T CONFIGURE YOUR CHEMISTRY TO
SUIT YOUR EQUIPMENT - SELECT THE SIMULAR TO SUIT YOUR
CHEMISTRY.SpecificationTurnkey systems:
For safe and efficient scale up, it is essential that your tools
simulate your plant as closely as possible. In addition it is
important that as much information and insight as possible about
the process be obtained. As such the options, upgrades and
flexibility offered by the SIMULAR are almost limitless, and we put
them all together in a turnkey and dedicated solution.Reactors:
The standard reactor is a 1 litre glass, atmospheric pressure
system. Optional volumes range from 0.2 to 20 litres in glass,
stainless steel or resistant alloy, with pressure ratings up to 200
bar. Specialist geometries and custom designed vessels are
available to simulate real plant conditions.Feeds:
Reagent Feeds - Gas, liquid and solids feeds are all available
using a variety of application dependent techniques. Standard
liquid feeds are pump and balance combinations, but options include
syringe pumps for low flow rate feeds and pressurised vessels for
faster rates and/or highly volatile reagents.Gas feeds can be
controlled via constant reactor pressure, bottle/balance
combinations or even mass flow control. Finally automated solids
addition is also made possible using a screw feed system developed
exclusively by HEL.Operating Range:
Pressure - HEL offer a range of options for the study of reactions
under pressure including 6 and 12 bar glass reactors, 60 bar
stainless steel with a number of other alloys and specialist
material options. We even produce systems that operate at up to 200
bar reactor pressure.
Temperature - By using commercially available heater/chiller
systems, we can offer you the temperature range you need, between
-80 and over 350¡£C, with precision of better than +/-0.1¡£C. These
systems also offer a small foot print and emergency cooling is
available when required.Controls & Sensors:
Software and electronics allow a variety of inputs to be logged and
if necessary, used for feedback co

